A Review Study of Agarwood Oil and Its Quality Analysis

Authors

  • Nurlaila Ismail Faculty of Electrical Engineering,Universiti Teknologi MARA (UiTM), 40450 Shah Alam, Selangor
  • Nor Azah Mohd Ali Herbal Product Development Programme, Natural Products Division, Forest Research Institute Malaysia (FRIM), 52109 Kepong, Selangor, Malaysia
  • Mailina Jamil Herbal Product Development Programme, Natural Products Division, Forest Research Institute Malaysia (FRIM), 52109 Kepong, Selangor, Malaysia
  • Mohd Hezri Fazalul Rahiman Faculty of Electrical Engineering,Universiti Teknologi MARA (UiTM), 40450 Shah Alam, Selangor
  • Saiful Nizam Tajuddin Faculty of Industrial Science and Technology, Universiti Malaysia Pahang (UMP), Lebuhraya Tun Razak, 26300 Gambang, Pahang, Malaysia
  • Mohd Nasir Taib Faculty of Electrical Engineering,Universiti Teknologi MARA (UiTM), 40450 Shah Alam, Selangor

DOI:

https://doi.org/10.11113/jt.v68.2419

Keywords:

Grading, agarwood oil, chemical compounds, signal processing

Abstract

This paper presents an overview of analysis agarwood oil and its quality grading. The review suggested agarwood oil can be graded according to their chemical properties and so that there is a common standard recognized worldwide on grading the agarwood oil. Analysis based on chemical profiles is required to ensure that agarwood oil can be classified based on their respective classes or grades where the accurate results can be measured. Conventionally, the grading of agarwood oil is performed by trained human graders (sensory panels) depends on its physical appearance such as color, odor, high fixative and consumer perception. However, this method is limited due to human nose cannot accept many samples in one time and easily get fatigues especially when dealing with continuous production. The human sensory panel also limited in terms of subjectivity, poor reproducibility, time consumption and large labour expense. These are constraining factors in increasing agarwood oil trade and market penetration. 

Author Biography

  • Nurlaila Ismail, Faculty of Electrical Engineering,Universiti Teknologi MARA (UiTM), 40450 Shah Alam, Selangor
    A PhD student from faculty of Electrical Engineering, UiTM Shah Alam.

References

R. Naef. 2011. The Volatile and Semi-volatile Constituents of Agarwood, the Infected Heartwood of Aquilaria Species: A Review. Flavour and Fragrance Journal. 26: 73–87.

M. A. NorAzah, J. A. Majid, J. Mailina, A. A. Said, S. S. Husni, H. N. Hasnida, M. A. M. N. M. Arip, and Y. S. Chang. 2009. Profiles of selected supreme Agarwood oils from Malaysia. Herbal Globalisation: A New Paradigm for Malaysian Herbal Industry (MAPS 2008). 393–398.

W. Hidayat, A. Y. M. Shakaff, M. N. Ahmad, and A. H. Adom. 2010. Classification of Agarwood Oil Using an Electronic Nose. Sensors. 10: 4675–4685.

M. S. Najib, N. A. M. Ali, M. N. M. Arip, A. M. Jalil, and M. N. Taib. 2010. Classification of Agarwood region using ANN. IEEE Control and System Graduate Research Colloquium (ICSGRC 2011). 7–13.

M. S. Najib, N. A. M. Ali, M. N. M. Arip, A. M. Jalil, M. N. Taib, and N. Kasuan. 2010. Classification of Malaysian and Indonesian Agarwood using k-NN.

M. S. Najib, M. N. Taib, N. A. M. Ali, M. N. M. Arip, and A. M. Jalil. 2011. Classification of Agarwood Grades using ANN. International Conference on Electrical, Control and Computer Engineering.

N. A. B. Sidik. 2008. Comparison of Gaharu (Aquilaria Malaccensis) Essential Oil Composition Between Each Country. Bachelor of Chemical Engineering, Faculty of Chemical Engineering and Natural Resources, University Malaysia Pahang.

N. A. M.A., Y. S. Chang, M. J., A. S. A, A. M. J., S. H. S., N. H. H., and N. Y. Y. 2008. Comparison of Chemical Profiles of Selected Gaharu Oils from Peninsular Malaysia. The Malaysian Journal of Analytical Sciences. 12: 340.

A. K. Pravina. 2008. Application of Solid Phase Microextraction in Gaharu Essential Oil Analysis. Bachelor of Chemical Engineering, Faculty of Chemical Engineering and Natural Resources, Univerisiti Malaysia Pahang (UMP), Pahang.

M. Ishihara, T. Tsuneya, M. Shiga, and K. Uneyama. 1991. Three sesquiterpenes from agarwood. Phytochemistry. 30: 563–566.

M. Ishihara, T. Tsuneya, and K. Uneyama. 1993. Fragrant Sesquiterpenes from Agarwood. Phytochemistry. 33: 1147–1155.

M. Ishihara, T. Tsuneya, and K. Uneyama. 1991. Guaiane Sesquiterpenes from Agarwood. Phytochemistry. 30: 3343–3347.

M. Ishihara, T. Tsuneya, and K. Uneyama. 1993. Components of the Agarwood Smoke on Heating. Journal of Essential Oil Research. 5: 419–423.

M. Ishihara, T. Tsuneya, and K. Uneyama. 1993. Components of the Volatile Concentrate of Agarwood. Journal of Essential Oil Research. 5: 283–289.

S. N. Tajuddin. 2011. Resolution of Complex Sesquiterpene Mixture in Aqualaria Malaccensis (Gaharu) Volatile Oils Using Gas Chromatography Methods. PhD, Faculty of Industry and Science Technology (FIST), Universiti Malaysia Pahang (UMP).

P. Wetwitayaklung, N. Thavanapong, and J. Charoenteeraboon. 2009. Chemical Constituents and Antimicrobial Activity of Essential Oil and Extracts of Heartwood of Aquilaria crassna Obtained from Water Distillation and Supercritical Fluid Carbon Dioxide Extraction. Silpakorn University Science and Technology Journal. 3: 25–33.

M. Meier, B. Kohlenberg, and N. A. Braun. 2003. Isolation of Anisyl Acetone from Agarwood Oil. Journal of Essential Oil Research. 15: 54–56.

M. N. I. Bhuiyan, J. Begum, and M. N. H. Bhuiyan. 2008. Analysis of essential Oil of Eaglewood Tree (Aquilaria agallocha Roxb.) by Gas Chromatography Mass Spectrometry. Bangladesh Journal of Pharmacology. 4: 24–28.

P. Pripdeevech, W. Khummueng, and S. K. Park. 2011. Identification of Odor-active Components of Agarwood Essential Oils from Thailand by Solid Phase Microextraction-GC/MS and GC-O. Journal of Essential Oil Research. 23: 46–53.

H. F. Lim, A. M. A. Rashid, S. S. Lee, P. A. Fauzi, Y. S. Chang, Y. A. Zuhaidi, M. M. Parid, E. H. Lok, A. M. Farid, and M. A. N. Azah. 2010. Penanaman Aquilaria dan Penghasilan Gaharu di Malaysia. Forest Research Institute Malaysia (FRIM), Kepong, Malaysia 93.

N. A. Latif. 2009. Analysis volatile compound of Gaharu oil Composition via solid phase micro extraction (SPME). Bachelor of Chemical Engineering, Faculty of Chemical Engineering, Universiti Malaysia Pahang, Pahang.

X. L. Zhang, Y. Y. Liu, J. H. Wei, Y. Yang, Z. Zhang, J. Q. Huang, H. Q. Chen, and Y. J. Liu. 2012. Production of High-quality Agarwood in Aquilaria Sinensis Trees via Whole-tree Agarwood-induction Technology. Chinese Chemical Letters. 23: 727–730.

P. Tamuli, P. Boruah, S. C. Nath, and P. Leclercq. 2005. Essential Oil of Eaglewood Tree: A Product of Pathogenesis. Journal of Essential Oil Research. 17: 601–604.

N. A. Latif. 2009. Analysis volatile compound of Gaharu oil composition via solid phase micro extraction (SPME). Bachelor of Chemical Engineering, Faculty of Chemical & Natural Resources Engineering, University Malaysia Pahang.

H. P. Bais, B. Dattatreya, and G. Ravishankar. 2003. Production of volatile compounds by hairy root cultures of Cichorium intybus L under the Influence of Fungal Elicitors and Their Analysis Using Solid Phase Micro Extraction Gas Chromatography–Mass Spectrometry. Journal of the Science of Food and Agriculture. 83: 769–774.

R. J. Bryant and A. M. McClung. 2011. Volatile profiles of Aromatic and Non-aromatic Rice Cultivars using SPME/GC–MS. Food Chemistry. 124: 501–513.

W. Chen, P. Zhou, K. C. Wong-Moon, and N. S. Cauchon. 2007. Identification of Volatile Degradants in Formulations Containing Sesame Oil Using SPME/GC/MS. Journal of Pharmaceutical and Biomedical Analysis. 44: 450–455.

[28] A. Cimato, D. Dello Monaco, C. Distante, M. Epifani, P. Siciliano, A. M. Taurino, M. Zuppa, and G. Sani. 2006. Analysis of Single-cultivar Extra Virgin Olive Oils by Means of an Electronic Nose and HS-SPME/GC/MS Methods. Sensors and Actuators B: Chemical. 114: 674–680.

L. Jirovetz, G. Buchbauer, M. B. Ngassoum, and M. Geissler. 2002. Aroma Compound Analysis of Piper Nigrum and Piper Guineense Essential Oils From Cameroon Using Solid-Phase Microextraction–Gas Chromatography, Solid-Phase Microextraction–Gas Chromatography–Mass Spectrometry and Olfactometry. Journal of Chromatography A. 976: 265–275.

Z. Meng, W. Dan, R. Shao-Xiong, and P. Ling. 2011. Head-Space Solid Phase Microextraction and GC-MS Analysis of Aroma Compounds in Feijoa Sellowiana. In 2011 5th International Conference on Bioinformatics and Biomedical Engineering, (iCBBE). 1–4.

H. Reinhard, F. Sager, and O. Zoller. 2008. Citrus Juice Classification by SPME-GC-MS and Electronic Nose Measurements. LWT - Food Science and Technology. 41: 1906–1912.

M. H. F. Rahiman. 2009. System Identification of Steam Distillation Essential Oil Extraction System. Ph.D. dissertation, Universiti Teknologi MARA, Shah Alam.

N. Ismail, N. Tajjudin, M. H. F. Rahiman, and M. N. Taib. 2009. Modeling of Dynamic Response of Essential Oil Extraction Process. In 5th International Colloquium on Signal Processing & Its Applications, CSPA 2009. 298–301.

K. H. K. Hamid. 2011. Ed., Professional lecture: enhancing the world of fragrance through Malaysian Bio-Gaharu. Shah Alam, Selangor, Malaysia: University Publication Centre (UPENA), UiTM.

A. M. A. Rashid and Y. A. Zuhaidi. 2011. Eds., Tapping the wealth from Karas (Aquilaria malaccensis) tree. Selangor, Malaysia: Forest Research Institute Malaysia.

T. Nakanishi, E. Yamagata, K. Yoneda, and T. Nagashima. 1984. Three Fragrant Sesquiterpenes of Agarwood. Phytochemistry. 23: 2066–2067.

K. H. K. Hamid. 2011. Professorial Lecture: Enhancing The World of Fragrance Through Malaysian Bio-Gaharu, 1st ed. UiTM Shah Alam: University Publication Centre (UPENA).

S. N. Tajuddin and M. M. Yusoff. 2010. Chemical Composition of Volatile Oils of Aquilaria malaccensis (Thymeleaceae) from Malaysia. Natural Product Communications. 5: 1965–1968.

S. N. Tajuddin, N. S. Muhamad, M. A. Yarmo, and M. M. Yusoff. 2013. Characterization of the Chemical Constituents of Agarwood Oils from Malaysia by Comprehensive Two-Dimensional Gas Chromatography–Time-of-Flight Mass Spectrometry. Mendeleev Communications. 23: 51–52.

M. A. NorAzah, Y. S. Chang, J. Mailina, A. A. Said, J. A. Majid, S. S. Husni, H. N. Hasnida, and Y. N. Yasmin. 2008. Comparison of Chemical Profiles of Selected Gaharu Oils from Peninsular Malaysia. The Malaysian Journal of Analytical Sciences. 12: 338–340.

A. Barden, N. A. Anak, T. Mulliken, and M. Song. 2000. Heart of the Matter: Agarwood Use and Trade and CITES implementation for Aquilaria malaccensis. TRAFFIC International, Cambridge, UK.

N. H. Yusoff, M. M. Salleh, M. Yahaya, and M. R. Awang. 2006. The Use of Photoluminescence Spectra of TiO2 Nanoparticles Coated With Porphyrin Dye Thin Film for Grading Agarwood Oil. In Proceedings of ICSE2006. 193–197.

H. Takemoto, M. Ito, T. Shiraki, T. Yagura, and G. Honda. 2008. Sedative Effects of Vapor Inhalation of Agarwood Oil and Spikenard Extract and Identification of Their Active Components. J Nat Med. 62: 41–6.

M. A. NorAzah, N. Ismail, and M. N. Taib. 2012. Analysis of Agarwood oil (Aquilaria Malaccensis) based on GC-MS data. In 2012 IEEE 8th International Colloquium on Signal Processing and its Applications (CSPA). 470–473.

J. Pornpunyapat, P. Chetpattananondh, and C. Tongurai. 2011. Mathematical Modeling for Extraction of Essential Oil from Aquilaria Crassna by Hydrodistillation and Quality of Agarwood Oil. Bangladesh Journal of Pharmacology. 6: 18–24.

S. F. A. Rahman. 2009. Analysis of Agarwood Oil Composition Via Preparative Thin Layer Chromatography..

P. E. Keller. 1999. Mimicking Biology: Applications of Cognitive Systems to Electronic Noses. 447–451.

M. Maheshwari, T. Jain, R. Bates, and S. Bhattacharyya. 1963. Terpenoids—xli: Structure and Absolute Configuration of α-agarofuran, b-agarofuran and Dihydroagarofuran. Tetrahedron. 19: 1079–1090.

T. Yagura, N. Shibayama, M. Ito, F. Kiuchi, and G. Honda. 2005. Three Novel Diepoxy Tetrahydrochromones from Agarwood Artificially Produced by Intentional Wounding. Tetrahedron Letters. 46: 4395–4398.

A. Ortega, S. Marco, T. Sundic, and J. Samitier. 2000. New Pattern Recognition Systems Designed for Electronic Noses. Sensor and Actuators B. 69: 302–307.

M. S. Najib, M. U. Ahmad, P. Funk, M. N. Taib, and N. A. M. Ali. 2012. Agarwood classification: A Case-Based Reasoning approach based on E-nose. In 2012 IEEE 8th International Colloquium on Signal Processing and its Applications (CSPA). 120–126.

N. Barié, M. Bücking, and M. Rapp. 2006. A Novel Electronic Nose Based on Miniaturized SAW with SPME Enhanced Headspace-analysis and Sensor Arrays Coupled Its Use for Rapid Determination of Volatile Organic Compounds in Food Quality Monitoring. Sensors and Actuators B: Chemical. 114: 482–488.

C. Cevoli, L. Cerretani, A. Gori, M. F. Caboni, T. Gallina Toschi, and A. Fabbri. 2011. Classification of Pecorino Cheeses Using Electronic Nose Combined with Artificial Neural Network and Comparison with GC–MS Analysis of Volatile Compounds. Food Chemistry. 129: 1315–1319.

F. Che Harun, J. Taylor, J. Covington, and J. Gardner. 2009. An Electronic Nose Employing Dual-channel Odour Separation Columns with Large Chemosensor Arrays for Advanced Odour Discrimination. Sensors and Actuators B: Chemical. 141: 134–140.

M. A. Craven, J. W. Gardner, and P. N. Bartlett. 1996. Electronic noses_Development and Future Prospects. Trends in Analytical Chemistry. 15 (9).

R. Dutta, D. Morgan, N. Baker, J. W. Gardner, and E. L. Hines. 2005. Identification of Staphylococcus Aureus Infections in Hospital Environment: Electronic Nose Based Approach. Sensors and Actuators B: Chemical. 109: 355–362.

J. W. Gardner and P. N. Bartlett. 2000. Electronic Noses. Principles and Applications. Oxford University Press.

J. W. Gardner, H. W. Shin, and E. L. Hines. 2000. An Electronic Nose System to Diagnose Illness. Sensors and Actuators B: Chemical. 70: 19–24.

J. W. Gardner, H. W. Shin, E. L. Hines, and C. S. Dow. 2000. An Electronic Nose System for Monitoring the Quality of Potable Water. Sensors and Actuators B: Chemical. 69: 336–341.

G. E. Scarle, J. W. Gardner, M. J. Chappell, K. R. Godfrey, and M. J. Chapman. 2002. System Identification of Electronic Nose Data from Cyanobacteria Experiments. IEEE Sensors Journal. 2: 218–229.

S. Panigrahi, S. Balasubramanian, H. Gu, C. Logue, and M. Marchello. 2006. Neural-network-integrated electronic nose system for identification of spoiled beef. LWT - Food Science and Technology. 39: 135–145.

P. J. Hobbs, T. H. Misselbrook, and B. F. Pain. 1994. Assessment of Odours from Livestock Wastes by a Photoionization Detector, an Electronic Nose, Olfactometry and Gas Chromatography-Mass Spectrometry. J. Agric. Engng Res. 60: 137–144.

T. E. Acree. 1997. Peer Reviewed: GC/Olfactometry GC With a Sense of Smell. Analytical Chemistry. 69: 170A–175A.

Ã. Högnadóttir and R. L. Rouseff. 2003. Identification of Aroma Active Compounds in Orange Essence Oil Using Gas Chromatography–Olfactometry and Gas Chromatography–Mass Spectrometry. Journal of Chromatography A. 998: 201–211.

C. Deng, N. Liu, M. Gao, and X. Zhang. 2007. Recent Developments in Sample Preparation Techniques for Chromatography Analysis of Traditional Chinese Medicines. Journal of Chromatography A. 1153: 90–96.

J. Rohloff. 1999. Monoterpene composition of essential oil from peppermint (Mentha× piperita L.) with Regard to Leaf Position Using Solid-Phase Microextraction and Gas Chromatography/Mass Spectrometry Analysis. Journal of Agricultural and Food Chemistry. 47: 3782–3786.

E. Marengo, C. Baiocchi, M. Gennaro, P. Bertolo, S. Lanteri, and W. Garrone. 1991. Classification of Essential Mint Oils of Different Geographic Origin by Applying Pattern Recognition Methods to Gas Chromatographic Data. Chemometrics and Intelligent Laboratory Systems. 11: 75–88.

M. N. Taib, R. Andres, and R. Narayanaswamy. 1996. Extending the Response Range of an Optical Fibre Ph Sensor Using an Artificial Neural Network. Analytica Chimica Acta. 330: 31–40.

M. N. Taib, R. Adnan, and M. H. F. Rahiman. 2007. Practical System Identification. Shah Alam: Faculty of Electrical Engineering, UiTM.

C. DiStefano, M. Zhu, and D. Mindrila. 2009. Understanding and using Factor Scores: Considerations for the Applied Researcher. Practical Assessment, Research & Evaluation. 14: 1–11.

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Published

2014-04-22

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Science and Engineering

How to Cite

A Review Study of Agarwood Oil and Its Quality Analysis. (2014). Jurnal Teknologi, 68(1). https://doi.org/10.11113/jt.v68.2419