Effect of Stearic Acid on Rheological Properties of 316L Feedstock for Metal injection Moulding

Authors

  • Istikamah Subuki Faculty of Chemical Engineering, Universiti Teknologi MARA, 40450 Shah Alam, Selangor, Malaysia
  • Muhammad Hussain Ismail Centre for Advanced Materials Research (CAMAR), Faculty of Mechanical Engineering, Universiti Teknologi MARA, 40450 Shah Alam, Selangor, Malaysia
  • Amalina Amir Centre for Advanced Materials Research (CAMAR), Faculty of Mechanical Engineering, Universiti Teknologi MARA, 40450 Shah Alam, Selangor, Malaysia
  • Mohd Afian Omar AMREC, SIRIM Berhad, Lot 34, Jalan Hi-Tech 2/3, Kulim Hi Tech Park, 09000 Kulim, Kedah, Malaysia

DOI:

https://doi.org/10.11113/jt.v59.2587

Keywords:

Metal Injection Moulding, rheological properties, palm stearin, stearic acid, feedstock

Abstract

Stearic acid (SA) was used as an additive in the process of metal injection moulding (MIM). It was added to the wax/polymer mixture in order to modify the powder wetting, mould lubrication, mixture viscosity, residual stress and debinding behaviour. In this study, the effect of SA in feedstock formulation on mixing torque and rheological properties was investigated. Further, it’s correlation on the as-moulded and as-debound parts behaviour was also investigated. The results showed that addition of SA significantly reduced the mixing torque value and viscosity which correspond to decreasing in inter-particle friction. As a result, injection moulding could be carried out at a lower temperature to achieve sound moulded parts and increased the removal rate of binder during solvent extraction process. However, it seemed that increasing the SA had a little negative effect on the as-moulded density.

References

Rivers, R. D., Kokomo, I. 1978. U. S. Patent. 4113480.

Henmi, I., Noda, A., Ono, T. 1981. U. S. Patent. 4283360.

Wiech, Jr., R. E. & Calif, S. D. 1983. U. S. Patent. 4415528.

Chung, C. I., Cao, M. Y., Kupperblatt, G. B., & Rhee, B. O. 1990. Advances in Powder Metallurgy and Particulate Materials. 3: 193–211.

Omar, M. A., Ibrahim, R., Sidik, M. I., Mustapha, M. & Mohamad, M. 2003. Journal of Materials Processing Technology. 140: 397–400.

Lin, H. K. & Hwang, K. S. 1998. Acta Metal. 46(12): 4303–4309.

German, R. M. & Bose, A. 1997. Injection Molding of Metals and Ceramics. Metal Powder Industries Federation (MPIF)

Paul Lin, S. T. & German, R. M. 1994. Journals of Materials Science. 29: 5367–5373.

Merz, L., Rath, S., Piotter, V., Ruprecht, R. & Hausselt, J. 2004. Microsystem Technologies. 10.

Supati, R., Loh, N. H., Khor, K. A. & Tor, S. B. 2000. Materials Letter. 46: 109–114.

Tseng, W. J. 2000. Materials Science and Engineering. A289: 116–122.

Huang, B., Liang, S. & Qu, X. 2003. Journal of Material Processing Technology. 137: 132–137.

Ismail, M. H., Sidambe, A. T., Davies, H. A., Todd, I. 2010. Proceedings of World PM2010 Conference (EPMA), E. P. M. A. Florence Italy, European Powder Metallurgy Association (EPMA). 4: 347–354.

Subuki, I. 2010. Injection Moulding of 316L Stainless Steel Powder Using Palm Stearin Based Binder System,. PhD Thesis. UiTM.

Downloads

Published

2012-10-15

How to Cite

Effect of Stearic Acid on Rheological Properties of 316L Feedstock for Metal injection Moulding. (2012). Jurnal Teknologi (Sciences & Engineering), 59(2). https://doi.org/10.11113/jt.v59.2587