Synthesis and Characterization of Green Porous Carbons with Large Surface Area by Two Step Chemical Activation with KOH

Authors

  • Noor Shawal Nasri Sustainable Waste-to-Wealth Unit, UTM-MPRC Institute Oil & Gas, Energy Research Alliance, Universiti Teknologi Malaysia, 81310 UTM Johor Bahru, Johor, Malaysia
  • Mohammed Jibril Sustainable Waste-to-Wealth Unit, UTM-MPRC Institute Oil & Gas, Energy Research Alliance, Universiti Teknologi Malaysia, 81310 UTM Johor Bahru, Johor, Malaysia
  • Muhammad Abbas Ahmad Zaini Faculty of Chemical Engineering, Universiti Teknologi Malaysia, 81310 UTM Johor Bahru, Johor, Malaysia
  • Rahmat Mohsin Sustainable Waste-to-Wealth Unit, UTM-MPRC Institute Oil & Gas, Energy Research Alliance, Universiti Teknologi Malaysia, 81310 UTM Johor Bahru, Johor, Malaysia
  • Hamza Usman Dadum Sustainable Waste-to-Wealth Unit, UTM-MPRC Institute Oil & Gas, Energy Research Alliance, Universiti Teknologi Malaysia, 81310 UTM Johor Bahru, Johor, Malaysia
  • Ahmed Murtala Musa Sustainable Waste-to-Wealth Unit, UTM-MPRC Institute Oil & Gas, Energy Research Alliance, Universiti Teknologi Malaysia, 81310 UTM Johor Bahru, Johor, Malaysia

DOI:

https://doi.org/10.11113/jt.v67.2787

Keywords:

Adsorbent, coconut shell, micropores, synthesis, chemical activation, potassium hydroxide

Abstract

Porous carbons were synthesized from coconut shell using chemical activation by potassium hydroxide (KOH). N2 adsorption isotherm analysis for BET surface area and pore volume of the synthesized porous carbon were carried out. The Langmuir surface area, BET surface area and pore volume are 1646 m2/g, 1353 m2/g and 0.6 cm3/g, respectively. From the FTIR analysis, hydroxyls, alkenes, carbonyls and aromatics functional groups were identified. The proximate and ultimate analysis shows high percentage of carbon and less ash content which indicates a good precursor material for porous carbon. The carbonization temperature and time were also varied to observe their effect on the yield of char, with carbonization at 7000C for 2 h having highest yield of 32%.

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Published

2014-03-15

How to Cite

Synthesis and Characterization of Green Porous Carbons with Large Surface Area by Two Step Chemical Activation with KOH. (2014). Jurnal Teknologi (Sciences & Engineering), 67(4). https://doi.org/10.11113/jt.v67.2787